A 100% Water Mobile Phase HPLC-PDA Analysis of Selected Neonicotinoid Insecticides
Journal Title: JOURNAL OF ADVANCES IN CHEMISTRY - Year 2014, Vol 10, Issue 9
Abstract
This paper describes a reserved-phase HPLC method for detecting frequently-used neonicotinoid insecticides, acetamiprid (ATP) and imidacloprid (ICP), using an isocratic 100 % water mobile phase. Chromatographic separations were performed an Inertsil® WP300 C4 with water mobile phase and a photodiode-array detector. The total run time was < 7 min. The system suitability was well within the international acceptance criteria.  The detection limits were 0.013 μg ml-1 for ATP and 0.015 μg ml-1 for ICP, respectively. A harmless HPLC method for simultaneous detecting ATP and ICP was developed and may be further applied to the quantification in foods. Â
Authors and Affiliations
Naoto Furusawa
Keywords
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- EP ID EP652788
- DOI 10.24297/jac.v10i9.878
- Views 175
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