Determination of ethyl bromide in the workplace air by gas chromatography with mass detection (GC-MS)

Journal Title: Podstawy i Metody Oceny Środowiska Pracy - Year 2013, Vol 29, Issue 1

Abstract

A new procedure has been developed for the assay of ethyl bromide with gas chromatography with mass detection (GC-MS). The method is based on the adsorption of ethyl bromide on petroleum charcoal and desorption with 10% acetone in toluene. The resulting solutions are analysed with GC-MS.The working range of this analytical method is from 10 to 1500 µg/ml (1 to 150 mg/m[sup]3[/sup] for a 10-L air sample). Limit of quantification: 1.76 µg/ml.The developed method of determining ethyl bromide has been recorded as an analytical procedure, which is available in the Appendix.

Authors and Affiliations

WIKTOR WESOŁOWSKI , MAŁGORZATA KUCHARSKA , JAN GROMIEC

Keywords

Related Articles

Methanol. Chromatographic determination in workplace air

This article presents a method for analysing methanol with gas chromatography with flame ionization detection (GC-FID). This method is based on adsorbing methanol vapors on active charcoal and desorbing the solvent mixtu...

Lead and its inorganic compounds – method of determining in workplace air

Lead is a soft, flexible and grey metal. In industry, it is used as an ingredient of many alloys, jacketing cables, screens protecting against ionizing radiation and battery plates. Lead and its compounds are highly toxi...

Phenolphthalein – inhalable fraction. Documentation of proposed values of occupational exposure limits (OELs)

Phenolphthalein is a colorless and odorless crystalline solid; in a powdered form white or pale yellow. It is nonvolatile, practically insoluble in water, but it dissolves in ethanol. Phenolphthalein is not known to occu...

1,1-Dichloroethene. Documentation

1,1-Dichloroethene (vinylidene chloride) is a low temperature boiling liquid with a sweet scent. 1,1-Dichloroethene is used as a chemical intermediate (usually with vinyl chloride) in the production of thermoplastic resi...

Butyl acetate (n-butyl) and its isomers – sec-butyl acetate and isobutyl acetates. Documentation of proposed values of occupational exposure limits (OELs)

Butyl acetates, or acetic acid esters and a suitable butyl alcohol, are four compounds with identical molecular formulas which differ from each other by sequence of bonding of atoms. These are n-butyl acetate with a stra...

Download PDF file
  • EP ID EP224572
  • DOI -
  • Views 124
  • Downloads 0

How To Cite

WIKTOR WESOŁOWSKI, MAŁGORZATA KUCHARSKA, JAN GROMIEC (2013). Determination of ethyl bromide in the workplace air by gas chromatography with mass detection (GC-MS). Podstawy i Metody Oceny Środowiska Pracy, 29(1), 101-112. https://europub.co.uk./articles/-A-224572