Cf/C composites: correlation between CVI process parameters and Pyrolytic Carbon microstructure

Journal Title: Frattura ed Integrità Strutturale - Year 2014, Vol 8, Issue 30

Abstract

 Chemical Vapour Infiltration (CVI) technique has been long used to produce carbon/carbon composites. The Pyrolytic Carbon (Py-C) matrix infiltrated by CVI could have different microstructures, i.e. Rough Laminar (RL), Smooth Laminar (SL) or Isotropic (ISO). These matrix microstructures, characterized by different properties, influence the mechanical behaviour of the obtained composites. Tailoring the process parameters, it is possible to direct the infiltration towards a specific Py-C type. However, the factors, influencing the production of a specific matrix microstructure, are numerous and interconnected, e.g. temperature, pressure, flow rates etc. Due to the complexity of the physical and chemical phenomena involved in CVI process, up to now it has not been possible to obtain a general correlation between CVI process parameters and Py–C microstructure. This study is aimed at investigating the relationship between infiltration temperature and the microstructure of obtained Py-C, for a pilot - sized CVI/CVD reactor. Fixing the other process parameters and varying only the temperature, from 1100°C to 1300°C, the Py-C infiltration was performed on fibrous preforms. Polarized light microscopy, with quantitative measurements of average extinction angle (Ae), and Raman spectroscopy were used to characterize the obtained Py-C microstructures.

Authors and Affiliations

F. Burgio, P. Fabbri, G. Magnani, M. Scafè, L. Pilloni, A. Brentani, T. Salzillo

Keywords

Related Articles

 The effect of thickness on out-of-plane constraint in terms of the T-stress

 The plastic zone is theoretically and numerically analyzed for various combinations of the nonsingular terms xx T to zz T ratios in connection with specimen thickness under mode I loading. The plastic zone size d...

 A research on detecting and recognizing bridge cracks in complex underwater conditions

 The method aims to recognize and extract the characteristic parameters of bridge cracks based on images of the cracks obtained through the application of preprocessing technologies, such as graying, graphical enh...

Propagazione di fratture longitudinali in gasdotti caratterizzati da bassa duttilità

 Il presente lavoro propone l’analisi di propagazione di una frattura fragile longitudinale di un gasdotto interrato basata sulla valutazione dell’energy release rate. Viene illustrata l’implementazione della sudd...

Evaluation of stress intensity factor of multiple inclined cracks under biaxial loading

 A finite rectangular plate of unit thickness with two inclined cracks (parallel and non parallel) under biaxial mixed mode condition are modelled using finite element method. The finite element method is used for d...

Download PDF file
  • EP ID EP121640
  • DOI -
  • Views 60
  • Downloads 0

How To Cite

F. Burgio, P. Fabbri, G. Magnani, M. Scafè, L. Pilloni, A. Brentani, T. Salzillo (2014).  Cf/C composites: correlation between CVI process parameters and Pyrolytic Carbon microstructure. Frattura ed Integrità Strutturale, 8(30), 68-74. https://europub.co.uk./articles/-A-121640