STUDY ON THE MODIFICATION OF ISOBUTYLATED PRODUCTS OF P – METHYLPHENOL DICYCLOPENTADIENE BY ACRYLATE
Journal Title: Topics in Chemical & Material Engineering (TCME) - Year 2018, Vol 1, Issue 1
Abstract
A new method of modification of polyphenol antioxidant was explored. CPL esterification was synthesized by esterification with acrylic acid, phosphorus oxychloride and triethylamine. A single factor experiment was carried out to explore the effects of different raw materials, raw material quality ratio and reaction temperature on polyphenol antioxidants. Find the best reaction conditions. The melting point and saponification values were used to characterize the resulting esters, which were analyzed experimentally. The optimum process conditions are as follows: m (polyphenol compound): m (acrylic acid): m (phosphorus oxychloride): m (triethylamine) =18:2:4:3, the optimum reaction temperature is 79℃, and the heat preservation reaction time is 2.5h. Under this technological condition, esterification. The esterification rate 88 to 90%. After being modified, esterified products with different melting points and saponification values can be used as alternatives for new antioxidants in the future. Different natures of esterification can be applied in different fields in the future
Authors and Affiliations
Yuting Gao, Chuanbo Dai, Tingting Zhao, Jianhua Qi
Keywords
Related Articles
- EP ID EP414302
- DOI 10.26480/icnmim.01.2018.179.182
- Views 44
- Downloads 0
CORN COB POLYMER FLOCCULANT PREPARATION METHOD AND ITS APPLICATION IN ORGANIC WASTE WATER TREATMENT
In this paper, the corn cob was modified to prepare cellulose xanthogen with flocculation. A comparative experiment was conducted on the flocculating adsorption effect of the finished product. Experiments show the best e...
SLUDGE AUTOMATIC RECOVERY SYSTEM IN THE STEEL SEDIMENTATION POND
A lot of sludge will be produced in steel and other industrial production. The precipitation of iron sludge will be recycled again after treatment. In order to make a voluntary recall at a certain depth. According to Tan...
THE SERVO-CONTROL TECHNOLOGY OF MULTI-DOF ROBOT BASED ON CANBUS
A study for servo-control technology of multi-DOF robot is proposed, the structure of control system and principle of servo driver circuits for DC motor with low inertia presented. The experiment results are reported, in...
STUDY ON THE EXTRACTION OF PIGMENT FROM FRUIT OF ROSA DAVURICA PALL.WITH MICROWAVE COENZYME METHOD AND ITS STABILITY AND INOXIDIZABILITY
To explore the best extracting process, stability and antioxidation activity in vitro of pigment extracted from fruit of Rosa davurica Pall., orthogonal design method was applied to determine optimal results. Antioxidant...
DESIGN OF EXPERIMENTAL SYSTEM FOR AUTOMATIC INSTRUMENT BASED ON STEP
An instrument experimental system is designed, which is used to measure several big parameters in the industrial process. The measuring parameters of the automatic experimental installation include liquid level, flow, te...