Syntheses and Characterization of 1-D Titanium Glycolate microstructures: Effect of Dilution and Addition type on the Morphology of microstructures
Journal Title: International Journal of Engineering and Science Invention - Year 2017, Vol 6, Issue 11
Abstract
Titanium glycolate is synthesized by the reaction of titanium butoxide with monoethylene glycol. This is a quick and convenient method for the preparation of titanium glycolate; the glycol acts as both reactant as well as solvent in the reaction. None of earlier studies reported in prior arthave attempted a detailed investigation into factors influencing the transition of the multidimensional Ti glycolate structure to the one dimensional (1-D) Ti glycolate structure, though previous studies report the formation of titanium glycolates possessing different shape and size characteristics (i.e. micro-rods, whiskers, wires, and so forth) at varying syntheses conditions. This paper reports the transition of multi-dimensional to 1-D Ti glycolate structures (transition from micro-rods to nanowires) through a detailed investigation of key process parameters which direct the formation of a 1-D structure. The characterization of the as-prepared titanium glycolates has been conducted using various analytical techniques viz. Scanning electron microscopy (SEM), Thermo-gravimetric analyses (TGA, TGA-MS); Inductively Coupled Plasma – Optical Emission spectroscopy (ICP-OES), Fourier Transform Infrared spectroscopy (FT-IR) and Elemental analysis (CHNS).
Authors and Affiliations
Shilpa Shinde, Abha Dhomane, Mahesh Subramaniyam
Keywords
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