Synthesis and crystal structure of N1-tosylacetylamidrazone
Journal Title: JOURNAL OF ADVANCES IN CHEMISTRY - Year 2014, Vol 10, Issue 2
Abstract
The condensation of two molar equivalents of N1-tosylhydrazonate 1 with one molar equivalent of 1,2-diaminoethane give birth to amidrazone in good yields. The structure of the synthesized compound was identified by X-ray diffraction, IR spectroscopy and nuclear magnetic resonance.Â
Authors and Affiliations
Salwa Hamzaoui, Bochra Ben Salah, Awatef Rekik, Mohamed Kossentini
VALIDATED IC METHOD FOR DETERMINATION OF CONTENTS OF RESIDUAL AMINO GUANIDINE IN LAMOTRIGINE DRUG SUBSTANCES WITH SUPPRESSED CONDUCTIVITY DETECTOR
This paper describes a validated method for the quantification of amino guanidine in Lamotrigine drug substances and their intermediates using Ion Chromatography (IC), with out any dervitization process. It was analysed...
Conservative liquids based on synthetic petroleum acids salts and aliphatic nitro-compounds
Synthetic oil acids (SOA) salts and nitroderivatives of high olefins C14 as oil-soluble corrosion inhibitors for mild steel in various mediums was synthesized. On the bases of turbine oil T-30 was prepared composition of...
Study on the Technology Conditions of Flue Gas Desulfurization with Organic Solvent
The technology experiment on Flue Gas Desulfurization (FDG) by DMSO method is studied in this paper, and the desulfurization efficiency is set out in various conditions. The results show that the desulfurization efficien...
Microstructure and Wear Behaviour of Aluminium Metal Matrix Composites Reinforced With Mg-Sic-TiO2-flyash
Al6061 was particulate with various reinforcement composite metal matrix materials adding different matrices using stir casting method. Reinforcement of hybrid composites used to various kinds of applications such as goo...
Synthesis and Characteristic of Precipitated Nano-Silica
The reaction of precipitation of amorphous silicon dioxide from aqueous solution of sodium silicate and sulfuric acid has been studied. The factors affecting the precipitation process of the sodium silicate solution such...