Synthesis, Characterization And Crystallographic Features Of Zirconium Molybdo-Pyrophosphate As A Composite Material
Journal Title: International Journal of Innovative Research & Growth - Year 2018, Vol 6, Issue 6
Abstract
Abstract A three inorganic ion exchange materials zirconium phosphate,zirconium molybdateand zirconium molybdo-pyrophosphate have been synthesized under identical conditions. Structures of these materialswere established by chemical analysis,X-ray diffraction, thermo-gravimetric and differential thermal analyses,fourier transform infrared spectroscopy and X-ray fluorescence analysis.From the data obtained the synthesized materials can be written as (Zr1.15PO4.8.3H2O)for zirconium phosphate with an amorphous structure and (Zr1.18Mo6.7.2H2O) and(Zr1.7MoPO7.2.3H2O) for zirconium molybdate and zirconium molybdo-pyrophosphate, respectively, with the semicrystalline structures. The data obtained from X-ray peak broadening analysis was used to evaluate the crystallite size and lattice strain by Scherer’s formula and Williamson-Hall (W.H) analyses. The chemical stability of these materials has been investigated in water and acidic media.The ion exchange capacity of zirconium molybdo-pyrophosphate for Pb2+ and Cd2+ ions have been studied at different heating temperatures.
Authors and Affiliations
Keywords
Related Articles
- EP ID EP620422
- DOI 10.26671/IJIRG.2018.6.6.101
- Views 158
- Downloads 0
Rectangular Patch Antenna With EBG Enabled DGS For UWB Applications
Abstract The versatility is only in the inclusion of multiple band of operation in wireless technology, while the patch antennas are the most crucial key factors of this mode of communication. Patch antennas have a rapi...
Leaf Extract Assisted Synthesis Of Titanium Doped Tin Nanoparticle, Determination Of Ph & Electrical Conductivity And Recommendation Of Fertilizer
Abstract In this research paper we introduce leaf extract mediated synthesis of Titanium doped tin nanoparticle .Here Barmuda grass used as a bioreducing agent. This work reports a simple, novel, cost effective and eco-f...
Onion – Health Benefits
Abstract Onion is a part of allium family of vegetable and it has been cultivated for centuries for their flavors, characteristics and their medicinal properties. In past few years, onion production has increased by 25%...
A Study Of Pulsar: Interference Of Neutron Stars And Black Holes
Abstract Though there have been so many claims and counter claims but the first pulsar was discovered in 1967, quite accidentally, by Anthony Hewish and his co-workers notable, Miss J. Bell, at Cambridge. Hewish and his...
Sensitivity Analysis Of Inventory Model For Deteriorating Items With On-Hand Inventory Dependent Demand Rate And Infinite Production Rate Without Shortages
Abstract A deterministic inventory model for deteriorating items is considered. The rate of demand is variable and it is on-hand inventory dependent. Rate of replenishment is instantaneous. Shortages are not allowed. The...